Comprehensive analysis of heat treatment effects on PLA-wood biocomposites


Bakirci A., Turan M. K., KARPAT F.

Rapid Prototyping Journal, vol.31, no.9, pp.1893-1904, 2025 (SCI-Expanded, Scopus) identifier identifier

  • Publication Type: Article / Article
  • Volume: 31 Issue: 9
  • Publication Date: 2025
  • Doi Number: 10.1108/rpj-01-2025-0040
  • Journal Name: Rapid Prototyping Journal
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, ABI/INFORM, Aerospace Database, Communication Abstracts, Compendex, INSPEC, Metadex, Civil Engineering Abstracts
  • Page Numbers: pp.1893-1904
  • Keywords: Additive manufacturing, Bio composite, Heat treatment, Mechanical properties, PLA-wood, Temperature, Visual properties
  • Bursa Uludag University Affiliated: Yes

Abstract

Purpose: This study aims to investigate the effects of heat treatment on the mechanical and visual properties of PLA-wood samples. Three different heating temperatures and three different durations were applied to determine their impact on tensile strength, hardness, moisture resistance, dimensional stability, surface quality and visual appearance. Design/methodology/approach: Samples were designed according to ASTM standards and produced via additive manufacturing. A full factorial experimental design was used. A total of 11 experimental groups were created: one untreated, one dried-only and nine heat-treated. Mechanical and physical evaluations included tensile testing, Shore D hardness, surface roughness, moisture absorption and visual color changes using a custom-built low-cost colorimeter developed specifically for this study. Findings: Heat treatment improved mechanical strength and moisture resistance of PLA-wood. The highest tensile strength was achieved at 100 °C for 90 min, showing a 12.8% increase compared to the untreated group. Heat treatment increased hardness and brittleness while reducing elongation and moisture absorption. Dimensional changes stabilized after 100 °C for 90 min, and color generally darkened with increasing temperature. These findings indicate that heat treatment is effective for improving the performance and appearance of PLA-wood composites. Originality/value: This is one of the most comprehensive heat treatment studies on PLA-wood in the literature, incorporating five distinct testing methods. A novel, low-cost colorimeter was developed for visual analysis. The results contribute significantly to the limited body of work on PLA-wood biocomposites and offer guidance for enhancing their functional and aesthetic properties through post-processing.