OPTIMIZATION OF HEMP FABRIC NATURAL DYEING IN SUPERCRITICAL CARBON DIOXIDE MEDIUM BY RESPONSE SURFACE METHODOLOGY

EREN S., ÖZTÜRK M., Özenç A. A., EREN H. A.

Cellulose Chemistry and Technology, cilt.59, sa.7-8, ss.929-938, 2025 (SCI-Expanded, Scopus) identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 59 Sayı: 7-8
  • Basım Tarihi: 2025
  • Doi Numarası: 10.35812/cellulosechemtechnol.2025.59.78
  • Dergi Adı: Cellulose Chemistry and Technology
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Chemical Abstracts Core, Compendex
  • Sayfa Sayıları: ss.929-938
  • Anahtar Kelimeler: cellulose, hemp fabric, henna, natural dye, response surface methodology, scCO2 dyeing
  • Bursa Uludağ Üniversitesi Adresli: Evet

Özet

This study explores the dyeing of hemp fabric, a natural cellulosic material, using henna as a natural dye in a supercritical carbon dioxide (scCO2) medium. Given the significant environmental impact of conventional textile finishing, the research aims to provide an eco-friendly alternative to synthetic dyes. Response surface methodology (RSM) was applied to optimize dyeing conditions, focusing on temperature, pressure, and time. The dyed samples were evaluated in terms of color fastness properties to assess the dye uptake and performance. The results showed that efficient dyeing was achieved without water, with maximum color strength (K/S value) at 120 °C, 21 MPa, and 90 minutes. The experimental K/S value closely matched the predicted value, validating the model's accuracy. Overall, the study demonstrated that natural dyeing of hemp in scCO₂ is feasible and sustainable, offering a waterless and environmentally friendly alternative for textile coloration.